材料期刊网

RELATIONSHIP BETWEEN PRIMARY MORPHOLOGY AND CRYSTAL STRUCTURE OF CARBIDES GROWING IN SUPERALLOYS

LIU Lin FU Hengzhi SHI Zhengxing Northwestern Polytechnical University , Xi'an , China Dr.LIU Lin Lecturer , Department of Applied Physics , Northwestern Polytechnical University , Xi'an 710072 , China

金属学报(英文版)

The SEM analysis of decply etched specimens of Ni-base superalloys K38 and K19H+Ta in- dicates that both the primary morphologies under normal growth conditions and the final morphologies near equilibrium of MC carbides are octahedral blocks.The classification of MC crystal faces by means of PBC(Periodic Bond Chains)theory confirms that{100}, {110}and{111}are F faces,and that{212}are S faces.The calculations of the attachment energy for each F face show that{111}are most easily appeared.It has also been inferred that one of the MC growth units is a coordination octahedron composed of one metal atom sur- rounded by six carbon atoms.The octahedral growth units can be attached to the growth sur- faces of MC carbides through laver stacking mechanism on the{111}faces.

关键词: carbide , null

FU105大功率广播发射管用碳化镧钼阴极研究

万小峰 , 张久兴 , 周文元 , 李湘波 , 周美玲

稀有金属材料与工程

研究了FU105大功率广播发射管用碳化镧钼阴极,参照碳化钍钨阴极FU105管的制备工艺,实现了镧钼阴极的碳化以及镧钼阴极FU105管的排气和老炼.通过镧钼阴极FU105管的性能测试,对碳化镧钼阴极的发射能力和稳定性进行了分析.结果认为:FU105管碳化镧钼阴极的发射能力可以达到碳化钍钨阴极的水平,但其稳定性还有待改进.

关键词: 镧钼阴极 , FU105发射管 , 碳化 , 稀土

[Pt(en)(5-Fu)2]Cl2配合物的合成及抗肿瘤活性

钟文远 , 崔永春 , 范春兰 , 胡智兴 , 李玛琳

贵金属 doi:10.3969/j.issn.1004-0676.2004.02.005

为寻求高效低毒的新型顺铂类抗肿瘤药物,用K2PtCl4、乙二胺(en)、氟尿嘧啶(5-Fu)为原料,设计合成了顺铂类似物[pt(en)(5-Fu)2]C12配合物,由元素分析、红外光谱和质谱分析初步证实了其化学结构,用改良MTT、SRB法,选用K562、A549、Bel-7402、BIU-87、Bcap-37细胞株对其进行体外抗肿瘤活性测定.结果表明,所合成的配合物除在浓度为0.01、0.1 μg/mL时对K562细胞株抗肿瘤活性大于顺铂和氟尿嘧啶外,其它情况下的抗肿瘤活性均小于顺铂和氟尿嘧啶.该配合物仍有进一步研究的价值.

关键词: 药学 , 铂(Ⅱ)配合物 , 合成 , 抗肿瘤活性

University of Science and Technology Beijing

JIA Shizhen University of Science and Technology Beijing , China.

材料科学技术（英）

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An Example of the Scientists—Congratulate Professor SHI Changxu on His Seventyth Birthday

DirectorsBoardofInstituteofMetalResearch , AcademiaSinica

金属学报(英文版)

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Department of Metallurgy and Materials Engineering of Chongqing University

YAN Guangting Chongqing University , Sichuan , China.

材料科学技术（英）

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Institute of Materials Science at Jilin University——A Brief Overview

WANG Yuming Institute of Materials Science , Jilin University , Changchun , 130023 , China

材料科学技术（英）

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表面包覆法合成的LiN0.8Co0.2O2材料的结构表征

刘欣艳 , 赵煜娟 , 夏定国

功能材料

LiNi0.8Co0.2O2是锂离子电池界公认的最有希望取代商业化正极材料LiCoO2的新型正极材料之一.本文所研究的复合正极材料LiNi0.8Co0.2O2是由细小的晶粒构成的球形颗粒,单一相,属于R3m空间群.对复合材料LiNi0.8Co0.2O2的Co-K和Ni-K的XANES分析可知,在600～850℃范围温度对于钴元素的影响不明显,而对于镍元素的影响比较显著,随着Ni-K边位置向高能量移动LiNi0.8Co0.2O2正极材料的放电容量升高.复合材料LiNi0.8Co0.2O2和LiNiO2的Ni-K边XANES相似,表明少量钴的引入对晶体结构的改变不是太多,但是峰的强度较高和峰的位置向高能量移动,表明钴Co对Ni的局域结构进行了调制.

关键词: LiNi0.8Co0.2O2 , XANES , 正极材料 , 局域结构

Abstracts of papers from Journal of University of Science and Technology Beijing

稀有金属（英文版）

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RF deflecting cavity design for bunch length measurement of photoinjector at Tsinghua University

中国物理C

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